James M. Miller

Chromatography 2e C

• Gebundenes Buch

Produktbeschreibung

Chromatography is a technique for analyzing or separating mixtures. The first edition of Chromatography: Concepts and Contrasts, published in 1988, was one of the first books to discuss all the different types of chromatography under one cover and is still very popular today. The second edition is updated to include new chapters on sampling and sample preparation, capillary electrophoresis and capillary electrochromatography (CEC), chromatography with mass spec detection, and industrial and governmental practices in regulated industries.

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The first edition of Chromatography: Concepts and Contrasts, published in 1988, was one of the first books to discuss all the different types of chromatography under one cover. The second edition continues with these principles but has been updated to include new chapters on sampling and sample preparation, capillary electrophoresis and capillary electrochromatography (CEC), chromatography with mass spec detection, and industrial and governmental practices in regulated industries.
_ Covers extraction, solid phase extraction (SPE), and solid phase microextraction (SPME), and introduces mass spectrometry.
_ Updated with the latest techniques in chromatography.
_ Discusses both liquid chromatography (LC) and gas chromatography (GC).

Produktdetails

• Verlag: Wiley & Sons
• Artikelnr. des Verlages: 14647207000
• 2. Aufl.
• Seitenzahl: 520
• Erscheinungstermin: 1. November 2004
• Englisch
• Abmessung: 240mm x 161mm x 32mm
• Gewicht: 855g
• ISBN-13: 9780471472070
• ISBN-10: 0471472077
• Artikelnr.: 13066495

Autorenporträt

I love children of all ages, and love reading to children. It is such a joy watching them grow, not only physically, but socially and mentally as well. I have worked many years with children and have loved every minute. I am always amazed how fast they learn, and I love being a part of that learning process. I have worked in the classroom and in many summer camps for kids and teens, helping them build confidence and self-esteem to conquer their tasks. I have kids of my own that I have encouraged to succeed and be independent. I love seeing everyone succeed, especially in their courage, certainty, and self-esteem.I love sailing, photography, hiking, camping, scuba diving, motorcycle riding, and spending time with family. If it involves water, outdoors or family, then chances are I love it.

Inhaltsangabe

Preface to Second Edition. Acknowledgments. Preface to the First Edition.
Symbols, Abbreviations, and Acronyms. 1 Impact of Industrial and Government
Regulatory Practices on Analytical Chromatography. 1.1 Locus of
Chromatography in Chemical Industry. 1.2 Governmental Organizations. 1.3
Nongovernmental Agencies. 1.4 Standards, Calibration, and NIST. 1.5 USP and
Other Pharmacopoeias. 1.6 International Guidelines for Analytical
Laboratories. 1.7 Final Comments. References. 2 Introduction to
Chromatography. 2.1 Brief History. 2.2 Definitions and Classifications. 2.3
Summary. References. 3 Band Broadening and Kinetics. 3.1 Configurations of
the Stationary Phase. 3.2 Rate Theory. References. 4 Physical Forces and
Interactions. 4.1 Intermolecular and Interionic Forces. 4.2 Size
Exclusion--Molecular Sieving. 4.3 Some Models. References. 5 Optimization
and the Achievement of Separation. 5.1 Kinetics and Zone Broadening. 5.2
Thermodynamics and Zone Migration. 5.2 Achievement of Separation. 5.4
Optimization of Separations. References. 6 Comparisons Between
Chromatographic Modes. 6.1 Gas Chromatography Compared to Liquid
Chromatography. 6.2 Supercritical Fluids and Supercritical Fluid
Chromatography. 6.3 Reduced Parameters. 6.4 Columnar and Planar
Configurations. References. 7 Gas Chromatography. 7.1 Early History,
Theories, and Classifications. 7.2 Instrumentation for Capillary GC. 7.3
Instrumentation for Packed-Column GC. 7.4 Stationary Phase. 7.5 Temperature
Effects. 7.6 Special Topics. 7.7 Summary and Evaluation. References. 8
Liquid Chromatography in Columns. 8.1 Introductory Classifications. 8.2
Classification of HPLC Modes. 8.3 Instrumentation. 8.4 Reversed-Phase
Method Development and Optimization. 8.5 RP-HPLC Alternatives for the
Pharmaceutical Industry. 8.6 Preparative LC. 8.7 Special Topics. 8.8
Summary and Evaluation. References. 9 Quantitation: Detectors and Methods.
9.1 Detectors. 9.2 Data Acquisition and Processing. 9.3 Quantitative
Analysis. References. 10 Chromatography with Mass Spectral Detection (GC/MS
and LC/MS). 10.1 Basics of Mass Spectrometry. 10.2 Gas ChromatographyrMass
Spectrometry. 10.3 Liquid ChromatographyrMass Spectrometry. 10.4 Other
Hyphenated Methods. 10.5 Summary. References. 11 Liquid Chromatography on
Plane Surfaces. 11.1 Paper Chromatography. 11.2 Thin-Layer Chromatography.
11.3 Other Topics. 11.4 Literature Summary and Applications. References. 12
Qualitative Analysis. 12.1 Retention Parameters. 12.2 Other Methods of
Qualitative Analysis. References. 13 Capillary Electrophoresis and
Capillary Electrochromatography 365 13.1 Principles of Electrophoresis.
13.2 Zone Electrophoresis. 13.3 Capillary Electrophoresis. 13.4 Capillary
Electrochromatography. References. 14 Sample Preparation. 14.1 Extraction.
14.2 Dialysis. 14.3 Derivatization. References. 15 Special Applications.
15.1 Multidimensional Chromatography. 15.2 Biological Applications. 15.3
Chiral Separations. 15.4 Other Topics. References. 16 Selection of a
Method. 16.1 Methods of Attack. 16.2 The Internet. 16.3 Experimental
Approach. 16.4 Summary. References. Some Internet Web Sites of Interest to
Chromatographers. Appendix A ICH Glossary. Appendix B. Index.

Rezensionen

"Professor Miller should be congratulated for the book...should be on the shelf of every practicing chromatographer...students taking separations science courses could also use it as their standard textbook." (Chromatographia, February 2005)

"Of course, I found a few mistakes, but not enough to criticize what is a useful, and, if not unique, at least a satisfying alternative approach to introducing a broad audience to the science, practice, and purpose of chromatography in a global context." (Chromatographia, August 2010)

...a practical, hands-on approach..." (CHOICE, July 2005)

"...an excellent introduction to all the chromatographic techniques for both the industrial practitioner and the...student because of its unified treatment, its modern approach, and up-to-date references." (Journal of the American Chemical Society, June 29, 2005)

"Professor Miller should be congratulated for the book...should be on the shelf of every practicing chromatographer...students taking separations science courses could also use it as their standard textbook." (Chromatographia, February 2005)