Roderick E Wasylishen, Sharon E Ashbrook, Stephen Wimperis

NMR of Quadrupolar Nuclei in Solid Materials

Ed. by Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis

• Gebundenes Buch

Produktbeschreibung

Many important materials do not contain spin-1/2 nuclei traditionally investigated by NMR spectroscopy and secondly, dissolving solid materials in a solvent may be impossible or may destroy the integrity of the material. All these obstacles can be overcome by NMR experiments at high-magnetic field strengths and investigating the properties of quadrupolar nuclei.

This Handbook gives an up-to-date account of NMR of quadrupoloar nuclei in the solid state. Each chapter of the Handbook has been prepared by an expert who has made significant contributions to our understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three Parts: A) Basic Principles of Quadrupolar NMR, B) Advanced Solid-State NMR Techniques to Investigate Quadrupolar Nuclei and C) Applications Involving NMR Studies of Quadrupolar Nuclei in Solids.

The first section provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar nuclei in solids. The second section presents cutting-edge techniques and methodology for employing these spectroscopic techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of biological samples to porous materials, catalysts, geological samples and high-temperature superconductors.

All these articles will be published on EMR: http://onlinelibrary.wiley.com/book/10.1002/9780470034590

Produktdetails

• EMR Books Vol.1
• Verlag: Wiley & Sons
• 1. Auflage
• Seitenzahl: 560
• Erscheinungstermin: 7. August 2012
• Englisch
• Abmessung: 254mm x 192mm x 30mm
• Gewicht: 1366g
• ISBN-13: 9780470973981
• ISBN-10: 0470973986
• Artikelnr.: 34437562

Autorenporträt

Roderick E. Wasylishen, Canada Research Chair in Physical Chemistry, Department of -Chemistry, Edmonton, Alberta, Canada. Sharon E. Ashbrook, Reader, School of Chemistry, University of St Andrews, UK. Stephen Wimperis, Professor, Department of Chemistry, Faculty of Physical Sciences, -University of Glasgow, UK.

Inhaltsangabe

Contributors ix Series Preface xiii Volume Preface xv Part A Basic
Principles 1 Quadrupolar Interactions Pascal P. Man 2 Quadrupolar Nuclei in
Solids Alexander J. Vega 3 Quadrupolar Coupling: An Introduction and
Crystallographic Aspects Sharon E. Ashbrook, Stephen Wimperis 4 Quadrupolar
Nuclei in Solids: Influence of Different Interactions on Spectra David L.
Bryce, Roderick E. Wasylishen Part B Advanced Techniques 5 Acquisition of
Wideline Solid-State NMR Spectra of Quadrupolar Nuclei Robert W. Schurko 6
Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei
in Solid-State NMR Thomas T. Nakashima, Roderick E. Wasylishen 7
Quadrupolar Nutation Spectroscopy Arno P. M. Kentgens 8 Dynamic Angle
Spinning Philip J. Grandinetti 9 Double Rotation (DOR) NMR Ray Dupree 10
MQMAS NMR: Experimental Strategies Jean-Paul Amoureux, Marek Pruski 11
STMAS NMR: Experimental Advances Sharon E. Ashbrook, Stephen Wimperis 12
Correlation Experiments Involving Half-Integer Quadrupolar Nuclei Michael
Deschamps, Dominique Massiot 13 Computing Electric Field Gradient Tensors
Josef W. Zwanziger Part C. Applications 14 Quadrupolar NMR to Investigate
Dynamics in Solid Materials Luke A. O'Dell, Christopher I. Ratcliffe 15
Alkali Metal NMR of Biological Molecules Gang Wu 16 Nitrogen-14 NMR Studies
of Biological Systems Luminita Duma 17 Oxygen-17 NMR Studies of Organic and
Biological Molecules Gang Wu 18 Oxygen-17 NMR of Inorganic Materials Sharon
E. Ashbrook, Mark E. Smith 19 Chlorine, Bromine and Iodine Solid-State NMR
David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell
20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related
Materials Frédéric Blanc, Leigh Spencer, Gillian R. Goward 21 Quadrupolar
NMR of Nanoporous Materials Mohamed Haouas, Charlotte Martineau, Francis
Taulelle 22 Quadrupolar NMR in the Earth Sciences Jonathan F. Stebbins 23
Quadrupolar NMR of Superconductors Nicholas J. Curro 24 Quadrupolar NMR of
Semiconductors James P. Yesinowski 25 Quadrupolar NMR of Metal Nuclides in
Biological Materials Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 26
Nuclear Waste Glasses: Insights from Solid-State NMR Scott Kroeker 27
Quadrupolar Metal NMR of Oxide Materials Including Catalysts Olga B.
Lapina, Victor V. Terskikh 28 Quadrupolar NMR of Intermetallic Compounds
Frank Haarmann Index