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In this thesis study, N-(4-(3-methyl-3-phenylcyclobutyl) thiazol-2-yl)formamide (C15H16N2OS) the single crystal structure consists of some compound groups such as thiazole, cyclobutene, and formamide groups were synthesized and characterized by IR, 1H NMR, and 13C NMR techniques. The molecular structure of the single crystal structure consisting of compounds that have a common usage area was analyzed by the X-ray diffraction technique. The compound C15H16N2OS was found to be in the monoclinic crystal system and the P21/c space group. The unit cell parameters of the molecular structure were obtained at a= 8.7592(7) Å, b= 5.7800(3) Å, c= 27.251(2) Å, =Gamma= 90°, and beta= 93.388(6)° from the X-ray diffraction results. When the bond parameters of the molecular structure were compared with similar studies, the bond parameters were found to be quite compatible. In the asymmetric unit, the molecular structure with the (x, y, z) symmetry code forms the chain forming structure by the dimeric form with the molecular structure with the (2-x, 1-y, -z) symmetry code.