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The book entitled "Review on Material Science Research Characterization Techniques(Vol.I)" has been written for upcoming research students. The book is enriched with introduction and theory part of promptly used material science experimental techniques like: Fourier Transform Infrared spectroscopy (FTIR), X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM), Hot Disc Thermal constant Analyzer, Dynamic Mechanical Analyzer (DMA), Electrometer and optical spectroscope for respective aspects, in brief. The book is saturated with well illustrated diagrams and much needed text. Language of the text is lucid and easy to understand.