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The present work was concerned with study of the blending ratio effect on the optical properties of the polymer systems involved [Poly(vinyl chloride) (PVC), Polystyrene (PS), Polymethylmethacrylate (PMMA)], binary blends [PS/PMMA, PVC/PMMA, PVC/PS] and ternary blends [PVC/PS/PMMA] at different concentrations. Also this work was concerned with study the effect of heat treatment of optical properties of polymer system involved [PVC/PS/PMMA] and binary blend with ratios, [50 %PS/50%PMMA, 50% PMMA/ 50% PVC and 50% PS /50% PVC].