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Recently invented 2D inorganic nanosheets are unique building blocks for the synthesis of nanohybrid materials. 2D nanosheets possess characteristics of large surface area, high morphological anisotropy, tunable chemical composition, and multiple redox active sites. Thus, 2D nanosheets-based nanohybrids have increased much attention as prospective candidates for supercapacitor electrodes. In this book focuses on preparing novel nanohybrids of 2D Nickel-Chromium Layered Double Hydroxide hybridized with 0D Polyoxometalates anions and 2D Graphene oxide nanosheets for supercapacitor application using a lattice engineering exfoliation-restacking route. The research analysis should be especially useful to the scientific community working on 2D inorganic nanosheets based nanohybrids for hybrid electrochemical energy storage devices.