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Provides an introduction to those needing to use infrared spectroscopy for the first time, explaining the fundamental aspects of this technique, how to obtain a spectrum and how to analyse infrared data covering a wide range of applications. _ Includes instrumental and sampling techniques _ Covers biological and industrial applications _ Includes suitable questions and problems in each chapter to assist in the analysis and interpretation of representative infrared spectra
Part of the ANTS (Analytical Techniques in the Sciences) Series.
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Provides an introduction to those needing to use infrared spectroscopy for the first time, explaining the fundamental aspects of this technique, how to obtain a spectrum and how to analyse infrared data covering a wide range of applications.
_ Includes instrumental and sampling techniques
_ Covers biological and industrial applications
_ Includes suitable questions and problems in each chapter to assist in the analysis and interpretation of representative infrared spectra
Part of the ANTS (Analytical Techniques in the Sciences) Series.
_ Includes instrumental and sampling techniques
_ Covers biological and industrial applications
_ Includes suitable questions and problems in each chapter to assist in the analysis and interpretation of representative infrared spectra
Part of the ANTS (Analytical Techniques in the Sciences) Series.
Produktdetails
- Produktdetails
- Analytical Techniques in the Sciences (AnTS)
- Verlag: Wiley & Sons
- 1. Auflage
- Seitenzahl: 248
- Erscheinungstermin: 30. Juli 2004
- Englisch
- Abmessung: 229mm x 152mm x 15mm
- Gewicht: 405g
- ISBN-13: 9780470854280
- ISBN-10: 0470854286
- Artikelnr.: 12921192
- Analytical Techniques in the Sciences (AnTS)
- Verlag: Wiley & Sons
- 1. Auflage
- Seitenzahl: 248
- Erscheinungstermin: 30. Juli 2004
- Englisch
- Abmessung: 229mm x 152mm x 15mm
- Gewicht: 405g
- ISBN-13: 9780470854280
- ISBN-10: 0470854286
- Artikelnr.: 12921192
Barbara Stuart, B.Sc. (Sydney), M.Sc. (Sydney), Ph.D. (London), D.I.C., MRACI, MRSC, Cchem After graduating with a B.Sc. degree from the University of Sydney in Australia, Barbara Stuart then worked as a tutor at this university. She also carried out research in the field of biophysical chemistry in the Department of Physical Chemistry and graduated with an M.Sc. in 1990. The author then moved to the UK to carry out doctoral studies in polymer engineering within the Department of Chemical Engineering and Chemical Technology at Imperial College (University of London). After obtaining her Ph.D. in 1993, she took up a position as a Lecturer in Physical Chemistry at the University of Greenwich in South East London. Barbara returned to Australia in 1995, joining the staff at the University of Technology, Sydney, where she is currently a Senior Lecturer in the Department of Chemistry, Materials and Forensic Science. She is presently conducting research in the fields of polymer spectroscopy, materials conservation and forensic science. Barbara is the author of three other books published by John Wiley and Sons, Ltd, namely Modern Infrared Spectroscopy and Biological Applications of Infrared Spectroscopy, both in the ACOL series of open learning texts, and Polymer Analysis in this current AnTS series of texts.
Series Preface. Preface. Acronyms, Abbreviations and Symbols. About the
Author. 1. Introduction. 1.1 Electromagnetic Radiation. 1.2 Infrared
Absorptions. 1.3 Normal Modes of Vibration. 1.4 Complicating Factors. 1.4.1
Overtone and Combination Bands. 1.4.2 Fermi Resonance. 1.4.3 Coupling.
1.4.4 Vibration-Rotation Bands. References. 2. Experimental Methods. 2.1
Introduction. 2.2 Dispersive Infrared Spectrometers. 2.3 Fourier-Transform
Infrared Spectrometers. 2.3.1 Michelson Interferometers. 2.3.2 Sources and
Detectors. 2.3.3 Fourier-Transformation. 2.3.4 Moving Mirrors. 2.3.5
Signal-Averaging. 2.3.6 Advantages. 2.3.7 Computers. 2.3.8 Spectra. 2.4
Transmission Methods. 2.4.1 Liquids and Solutions. 2.4.2 Solids. 2.4.3
Gases. 2.4.4 Pathlength Calibration. 2.5 Reflectance Methods. 2.5.1
Attenuated Total Reflectance Spectroscopy. 2.5.2 Specular Reflectance
Spectroscopy. 2.5.3 Diffuse Reflectance Spectroscopy. 2.5.4 Photoacoustic
Spectroscopy. 2.6 Microsampling Methods. 2.7 Chromatography-Infrared
Spectroscopy. 2.8 Thermal Analysis-Infrared Spectroscopy. 2.9 Other
Techniques. References. 3. Spectral Analysis. 3.1 Introduction. 3.2 Group
Frequencies. 3.2.1 Mid-Infrared Region. 3.2.2 Near-Infrared Region. 3.2.3
Far-Infrared Region. 3.3 Identification. 3.4 Hydrogen Bonding. 3.5 Spectrum
Manipulation. 3.5.1 Baseline Correction. 3.5.2 Smoothing. 3.5.3 Difference
Spectra. 3.5.4 Derivatives. 3.5.5 Deconvolution. 3.5.6 Curve-Fitting. 3.6
Concentration. 3.7 Simple Quantitative Analysis. 3.7.1 Analysis of Liquid
Samples. 3.7.2 Analysis of Solid Samples. 3.8 Multi-Component Analysis. 3.9
Calibration Methods. References. 4. Organic Molecules. 4.1 Introduction.
4.2 Aliphatic Hydrocarbons. 4.3 Aromatic Compounds. 4.4 Oxygen-Containing
Compounds. 4.4.1 Alcohols and Phenols. 4.4.2 Ethers. 4.4.3 Aldehydes and
Ketones. 4.4.4 Esters. 4.4.5 Carboxylic Acids and Anhydrides. 4.5
Nitrogen-Containing Compounds. 4.5.1 Amines. 4.5.2 Amides. 4.6
Halogen-Containing Compounds. 4.7 Heterocyclic Compounds. 4.8 Boron
Compounds. 4.9 Silicon Compounds. 4.10 Phosphorus Compounds. 4.11 Sulfur
Compounds. 4.12 Near-Infrared Spectra. 4.13 Identification. References. 5.
Inorganic Molecules. 5.1 Introduction. 5.2 General Considerations. 5.3
Normal Modes of Vibration. 5.4 Coordination Compounds. 5.5 Isomerism. 5.6
Metal Carbonyls. 5.7 Organometallic Compounds. 5.8 Minerals. References. 6.
Polymers. 6.1 Introduction. 6.2 Identification. 6.3 Polymerization. 6.4
Structure. 6.5 Surfaces. 6.6 Degradation. References. 7. Biological
Applications. 7.1 Introduction. 7.2 Lipids. 7.3 Proteins and Peptides. 7.4
Nucleic Acids. 7.5 Disease Diagnosis. 7.6 Microbial Cells. 7.7 Plants. 7.8
Clinical Chemistry. References. 8. Industrial and Environmental
Applications. 8.1 Introduction. 8.2 Pharmaceutical Applications. 8.3 Food
Science. 8.4 Agricultural Applications. 8.5 Pulp and Paper Industries. 8.6
Paint Industry. 8.7 Environmental Applications. References. Responses to
Self-Assessment Questions. Bibliography. Glossary of Terms. SI Units and
Physical Constants. Periodic Table. Index.
Author. 1. Introduction. 1.1 Electromagnetic Radiation. 1.2 Infrared
Absorptions. 1.3 Normal Modes of Vibration. 1.4 Complicating Factors. 1.4.1
Overtone and Combination Bands. 1.4.2 Fermi Resonance. 1.4.3 Coupling.
1.4.4 Vibration-Rotation Bands. References. 2. Experimental Methods. 2.1
Introduction. 2.2 Dispersive Infrared Spectrometers. 2.3 Fourier-Transform
Infrared Spectrometers. 2.3.1 Michelson Interferometers. 2.3.2 Sources and
Detectors. 2.3.3 Fourier-Transformation. 2.3.4 Moving Mirrors. 2.3.5
Signal-Averaging. 2.3.6 Advantages. 2.3.7 Computers. 2.3.8 Spectra. 2.4
Transmission Methods. 2.4.1 Liquids and Solutions. 2.4.2 Solids. 2.4.3
Gases. 2.4.4 Pathlength Calibration. 2.5 Reflectance Methods. 2.5.1
Attenuated Total Reflectance Spectroscopy. 2.5.2 Specular Reflectance
Spectroscopy. 2.5.3 Diffuse Reflectance Spectroscopy. 2.5.4 Photoacoustic
Spectroscopy. 2.6 Microsampling Methods. 2.7 Chromatography-Infrared
Spectroscopy. 2.8 Thermal Analysis-Infrared Spectroscopy. 2.9 Other
Techniques. References. 3. Spectral Analysis. 3.1 Introduction. 3.2 Group
Frequencies. 3.2.1 Mid-Infrared Region. 3.2.2 Near-Infrared Region. 3.2.3
Far-Infrared Region. 3.3 Identification. 3.4 Hydrogen Bonding. 3.5 Spectrum
Manipulation. 3.5.1 Baseline Correction. 3.5.2 Smoothing. 3.5.3 Difference
Spectra. 3.5.4 Derivatives. 3.5.5 Deconvolution. 3.5.6 Curve-Fitting. 3.6
Concentration. 3.7 Simple Quantitative Analysis. 3.7.1 Analysis of Liquid
Samples. 3.7.2 Analysis of Solid Samples. 3.8 Multi-Component Analysis. 3.9
Calibration Methods. References. 4. Organic Molecules. 4.1 Introduction.
4.2 Aliphatic Hydrocarbons. 4.3 Aromatic Compounds. 4.4 Oxygen-Containing
Compounds. 4.4.1 Alcohols and Phenols. 4.4.2 Ethers. 4.4.3 Aldehydes and
Ketones. 4.4.4 Esters. 4.4.5 Carboxylic Acids and Anhydrides. 4.5
Nitrogen-Containing Compounds. 4.5.1 Amines. 4.5.2 Amides. 4.6
Halogen-Containing Compounds. 4.7 Heterocyclic Compounds. 4.8 Boron
Compounds. 4.9 Silicon Compounds. 4.10 Phosphorus Compounds. 4.11 Sulfur
Compounds. 4.12 Near-Infrared Spectra. 4.13 Identification. References. 5.
Inorganic Molecules. 5.1 Introduction. 5.2 General Considerations. 5.3
Normal Modes of Vibration. 5.4 Coordination Compounds. 5.5 Isomerism. 5.6
Metal Carbonyls. 5.7 Organometallic Compounds. 5.8 Minerals. References. 6.
Polymers. 6.1 Introduction. 6.2 Identification. 6.3 Polymerization. 6.4
Structure. 6.5 Surfaces. 6.6 Degradation. References. 7. Biological
Applications. 7.1 Introduction. 7.2 Lipids. 7.3 Proteins and Peptides. 7.4
Nucleic Acids. 7.5 Disease Diagnosis. 7.6 Microbial Cells. 7.7 Plants. 7.8
Clinical Chemistry. References. 8. Industrial and Environmental
Applications. 8.1 Introduction. 8.2 Pharmaceutical Applications. 8.3 Food
Science. 8.4 Agricultural Applications. 8.5 Pulp and Paper Industries. 8.6
Paint Industry. 8.7 Environmental Applications. References. Responses to
Self-Assessment Questions. Bibliography. Glossary of Terms. SI Units and
Physical Constants. Periodic Table. Index.
Series Preface. Preface. Acronyms, Abbreviations and Symbols. About the
Author. 1. Introduction. 1.1 Electromagnetic Radiation. 1.2 Infrared
Absorptions. 1.3 Normal Modes of Vibration. 1.4 Complicating Factors. 1.4.1
Overtone and Combination Bands. 1.4.2 Fermi Resonance. 1.4.3 Coupling.
1.4.4 Vibration-Rotation Bands. References. 2. Experimental Methods. 2.1
Introduction. 2.2 Dispersive Infrared Spectrometers. 2.3 Fourier-Transform
Infrared Spectrometers. 2.3.1 Michelson Interferometers. 2.3.2 Sources and
Detectors. 2.3.3 Fourier-Transformation. 2.3.4 Moving Mirrors. 2.3.5
Signal-Averaging. 2.3.6 Advantages. 2.3.7 Computers. 2.3.8 Spectra. 2.4
Transmission Methods. 2.4.1 Liquids and Solutions. 2.4.2 Solids. 2.4.3
Gases. 2.4.4 Pathlength Calibration. 2.5 Reflectance Methods. 2.5.1
Attenuated Total Reflectance Spectroscopy. 2.5.2 Specular Reflectance
Spectroscopy. 2.5.3 Diffuse Reflectance Spectroscopy. 2.5.4 Photoacoustic
Spectroscopy. 2.6 Microsampling Methods. 2.7 Chromatography-Infrared
Spectroscopy. 2.8 Thermal Analysis-Infrared Spectroscopy. 2.9 Other
Techniques. References. 3. Spectral Analysis. 3.1 Introduction. 3.2 Group
Frequencies. 3.2.1 Mid-Infrared Region. 3.2.2 Near-Infrared Region. 3.2.3
Far-Infrared Region. 3.3 Identification. 3.4 Hydrogen Bonding. 3.5 Spectrum
Manipulation. 3.5.1 Baseline Correction. 3.5.2 Smoothing. 3.5.3 Difference
Spectra. 3.5.4 Derivatives. 3.5.5 Deconvolution. 3.5.6 Curve-Fitting. 3.6
Concentration. 3.7 Simple Quantitative Analysis. 3.7.1 Analysis of Liquid
Samples. 3.7.2 Analysis of Solid Samples. 3.8 Multi-Component Analysis. 3.9
Calibration Methods. References. 4. Organic Molecules. 4.1 Introduction.
4.2 Aliphatic Hydrocarbons. 4.3 Aromatic Compounds. 4.4 Oxygen-Containing
Compounds. 4.4.1 Alcohols and Phenols. 4.4.2 Ethers. 4.4.3 Aldehydes and
Ketones. 4.4.4 Esters. 4.4.5 Carboxylic Acids and Anhydrides. 4.5
Nitrogen-Containing Compounds. 4.5.1 Amines. 4.5.2 Amides. 4.6
Halogen-Containing Compounds. 4.7 Heterocyclic Compounds. 4.8 Boron
Compounds. 4.9 Silicon Compounds. 4.10 Phosphorus Compounds. 4.11 Sulfur
Compounds. 4.12 Near-Infrared Spectra. 4.13 Identification. References. 5.
Inorganic Molecules. 5.1 Introduction. 5.2 General Considerations. 5.3
Normal Modes of Vibration. 5.4 Coordination Compounds. 5.5 Isomerism. 5.6
Metal Carbonyls. 5.7 Organometallic Compounds. 5.8 Minerals. References. 6.
Polymers. 6.1 Introduction. 6.2 Identification. 6.3 Polymerization. 6.4
Structure. 6.5 Surfaces. 6.6 Degradation. References. 7. Biological
Applications. 7.1 Introduction. 7.2 Lipids. 7.3 Proteins and Peptides. 7.4
Nucleic Acids. 7.5 Disease Diagnosis. 7.6 Microbial Cells. 7.7 Plants. 7.8
Clinical Chemistry. References. 8. Industrial and Environmental
Applications. 8.1 Introduction. 8.2 Pharmaceutical Applications. 8.3 Food
Science. 8.4 Agricultural Applications. 8.5 Pulp and Paper Industries. 8.6
Paint Industry. 8.7 Environmental Applications. References. Responses to
Self-Assessment Questions. Bibliography. Glossary of Terms. SI Units and
Physical Constants. Periodic Table. Index.
Author. 1. Introduction. 1.1 Electromagnetic Radiation. 1.2 Infrared
Absorptions. 1.3 Normal Modes of Vibration. 1.4 Complicating Factors. 1.4.1
Overtone and Combination Bands. 1.4.2 Fermi Resonance. 1.4.3 Coupling.
1.4.4 Vibration-Rotation Bands. References. 2. Experimental Methods. 2.1
Introduction. 2.2 Dispersive Infrared Spectrometers. 2.3 Fourier-Transform
Infrared Spectrometers. 2.3.1 Michelson Interferometers. 2.3.2 Sources and
Detectors. 2.3.3 Fourier-Transformation. 2.3.4 Moving Mirrors. 2.3.5
Signal-Averaging. 2.3.6 Advantages. 2.3.7 Computers. 2.3.8 Spectra. 2.4
Transmission Methods. 2.4.1 Liquids and Solutions. 2.4.2 Solids. 2.4.3
Gases. 2.4.4 Pathlength Calibration. 2.5 Reflectance Methods. 2.5.1
Attenuated Total Reflectance Spectroscopy. 2.5.2 Specular Reflectance
Spectroscopy. 2.5.3 Diffuse Reflectance Spectroscopy. 2.5.4 Photoacoustic
Spectroscopy. 2.6 Microsampling Methods. 2.7 Chromatography-Infrared
Spectroscopy. 2.8 Thermal Analysis-Infrared Spectroscopy. 2.9 Other
Techniques. References. 3. Spectral Analysis. 3.1 Introduction. 3.2 Group
Frequencies. 3.2.1 Mid-Infrared Region. 3.2.2 Near-Infrared Region. 3.2.3
Far-Infrared Region. 3.3 Identification. 3.4 Hydrogen Bonding. 3.5 Spectrum
Manipulation. 3.5.1 Baseline Correction. 3.5.2 Smoothing. 3.5.3 Difference
Spectra. 3.5.4 Derivatives. 3.5.5 Deconvolution. 3.5.6 Curve-Fitting. 3.6
Concentration. 3.7 Simple Quantitative Analysis. 3.7.1 Analysis of Liquid
Samples. 3.7.2 Analysis of Solid Samples. 3.8 Multi-Component Analysis. 3.9
Calibration Methods. References. 4. Organic Molecules. 4.1 Introduction.
4.2 Aliphatic Hydrocarbons. 4.3 Aromatic Compounds. 4.4 Oxygen-Containing
Compounds. 4.4.1 Alcohols and Phenols. 4.4.2 Ethers. 4.4.3 Aldehydes and
Ketones. 4.4.4 Esters. 4.4.5 Carboxylic Acids and Anhydrides. 4.5
Nitrogen-Containing Compounds. 4.5.1 Amines. 4.5.2 Amides. 4.6
Halogen-Containing Compounds. 4.7 Heterocyclic Compounds. 4.8 Boron
Compounds. 4.9 Silicon Compounds. 4.10 Phosphorus Compounds. 4.11 Sulfur
Compounds. 4.12 Near-Infrared Spectra. 4.13 Identification. References. 5.
Inorganic Molecules. 5.1 Introduction. 5.2 General Considerations. 5.3
Normal Modes of Vibration. 5.4 Coordination Compounds. 5.5 Isomerism. 5.6
Metal Carbonyls. 5.7 Organometallic Compounds. 5.8 Minerals. References. 6.
Polymers. 6.1 Introduction. 6.2 Identification. 6.3 Polymerization. 6.4
Structure. 6.5 Surfaces. 6.6 Degradation. References. 7. Biological
Applications. 7.1 Introduction. 7.2 Lipids. 7.3 Proteins and Peptides. 7.4
Nucleic Acids. 7.5 Disease Diagnosis. 7.6 Microbial Cells. 7.7 Plants. 7.8
Clinical Chemistry. References. 8. Industrial and Environmental
Applications. 8.1 Introduction. 8.2 Pharmaceutical Applications. 8.3 Food
Science. 8.4 Agricultural Applications. 8.5 Pulp and Paper Industries. 8.6
Paint Industry. 8.7 Environmental Applications. References. Responses to
Self-Assessment Questions. Bibliography. Glossary of Terms. SI Units and
Physical Constants. Periodic Table. Index.