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This book explores the growth and characterization of nonlinear optical (NLO) materials, specifically pure and dye-doped L-histidine bromide, L-histidine cadmium chloride, and pure L-valine tin chloride. And provides a comprehensive overview of the preparation, crystal growth, and characterization of these materials using various techniques, including X-ray diffraction, UV-Vis spectroscopy, thermal analysis, and second harmonic generation (SHG) measurements. The author discusses the effect of doping with various organic dyes on the optical properties of the NLO materials and how they can be tailored to specific applications. Experimental results presented in the book show that the addition of dyes to the NLO materials improves their SHG efficiency, which makes them suitable for applications such as frequency conversion, optical modulation, and optical switching. The book also highlights the potential of these materials for applications in laser technology, telecommunications, and optical computing. Overall, "Growth and Characterization of NLO Materials with Dyes" is a valuable resource for researchers, scientists, and engineers working in the field of materials science and optics. The book provides an in-depth understanding of the growth and characterization of NLO materials with dyes and their potential applications in various fields. It also highlights the importance of developing new materials with improved properties to meet the demands of emerging technologies.