Handbook of Elemental Speciation (eBook, PDF)

Techniques and Methodology
Redaktion: Cornelis, Rita; Heumann, Klaus G.; Crews, Helen; Caruso, Joseph A.

• Format: PDF

Produktbeschreibung

This international collection of chapters comprehensively covers different aspects of procedures for speciation analysis at all levels starting from sample collection and storage, through sample preparation approaches to render the species chromatographable, principles of separation techniques used in speciation analysis, to the element specific detection. * International renowned editors and contributors * Includes coverage of electrochemical methods, biosensors for metal ions, radioisotope techniques and direct solid speciation techniques * Provides information on quality assurance and risk assessment, and speciation-relevant legislation Each chapter is a stand-alone reference covering a given facet of elemental speciation analysis written by an expert in a given field with the volume as a whole providing an excellent introductory text and reference handbook.

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Produktdetails

• Verlag: John Wiley & Sons
• Seitenzahl: 670
• Erscheinungstermin: 20. November 2003
• Englisch
• ISBN-13: 9780470868379
• Artikelnr.: 37299737

Autorenporträt

Rita Cornelis, Department of Analytical Chemistry, Ghent University, The Netherlands.

Inhaltsangabe

List of Contributors. Preface. Technical Abbreviations and Acronyms. 1
Introduction. 2 Sampling: Collection, Storage. 2.1 Sampling: Collection,
Processing and Storage of Environmental Samples. 2.2 Sampling of Clinical
Samples: Collection and Storage. 2.3 Food: Sampling with Special Reference
to Legislation, Uncertainty and Fitness for Purpose. 2.4 Sampling:
Collection, Storage - Occupational Health. 3 Sample Preparation. 3.1 Sample
Treatment for Speciation Analysis in Biological Samples. 3.2 Sample
Preparation Techniques for Elemental Speciation Studies. 3.3 Sample
Preparation - Fractionation (Sediments, Soils, Aerosols and Fly Ashes). 4
Separation Techniques. 4.1 Liquid Chromatography. 4.2 Gas Chromatography
and Other Gas Based Methods. 4.3 Capillary Electrophoresis in Speciation
Analysis. 4.4 Gel Electrophoresis for Speciation Purposes. 5 Detection. 5.1
Atomic Absorption and Atomic Emission Spectrometry. 5.2 Flow Injection
Atomic Spectrometry for Speciation. 5.3 Detection by ICP-Mass Spectrometry.
5.4 Plasma Source Time-of-flight Mass Spectrometry: a Powerful Tool for
Elemental Speciation. 5.5 Glow Discharge Plasmas as Tunable Sources for
Elemental Speciation. 5.6 Electrospray Methods for Elemental Speciation.
5.7 Elemental Speciation by Inductively Coupled Plasma-Mass Spectrometry
with High Resolution Instruments. 5.8 On-line Elemental Speciation with
Functionalised Fused Silica Capillaries in Combination with DIN-ICP-MS. 5.9
Speciation Analysis by Electrochemical Methods. 5.10 Future Instrumental
Development for Speciation. 5.11 Biosensors for Monitoring of Metal Ions.
5.12 Possibilities Offered by Radiotracers for Method Development in
Elemental Speciation Analysis and for Metabolic and Environmentally Related
Speciation Studies. 6 Direct Speciation of Solids. 6.1 Characterization of
Individual Aerosol Particles with Special Reference to Speciation
Techniques. 6.2 Direct Speciation of Solids: X-ray Absorption Fine
Structure Spectroscopy for Species Analysis in Solid Samples. 7
Calibration. 7.1 Calibration in Elemental Speciation Analysis. 7.2
Reference Materials. 8 Screening Methods for Semiquantitative Speciation
Analysis. 9 Risk Assessments/Regulations. 9.1 Environmental Risk Assessment
and the Bioavailability of Elemental Species. 9.2 Speciation and
Legislation. Index.