William Henderson, J. Scott Mcindoe
Mass Spectrometry of Inorganic and Organometallic Compounds (eBook, PDF)
Tools - Techniques - Tips
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William Henderson, J. Scott Mcindoe
Mass Spectrometry of Inorganic and Organometallic Compounds (eBook, PDF)
Tools - Techniques - Tips
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This is the first modern book to treat inorganic and organometallic mass spectrometry simultaneously. It is textbook and handbook in one; as a textbook it introduces the techniques and gives hints on how to apply the various techniques, as a handbook it lists all available ionization techniques for just about any given compound. The book also includes non-mathematical explanations of how modern MS instruments work Mass Spectrometry of Inorganic and Organometallic Compounds will inspire the synthetic inorganic and organometallic chemist with the confidence to apply some of the new techniques to their characterization problems.…mehr
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This is the first modern book to treat inorganic and organometallic mass spectrometry simultaneously. It is textbook and handbook in one; as a textbook it introduces the techniques and gives hints on how to apply the various techniques, as a handbook it lists all available ionization techniques for just about any given compound. The book also includes non-mathematical explanations of how modern MS instruments work Mass Spectrometry of Inorganic and Organometallic Compounds will inspire the synthetic inorganic and organometallic chemist with the confidence to apply some of the new techniques to their characterization problems.
Dieser Download kann aus rechtlichen Gründen nur mit Rechnungsadresse in A, B, BG, CY, CZ, D, DK, EW, E, FIN, F, GR, HR, H, IRL, I, LT, L, LR, M, NL, PL, P, R, S, SLO, SK ausgeliefert werden.
Produktdetails
- Produktdetails
- Verlag: John Wiley & Sons
- Seitenzahl: 292
- Erscheinungstermin: 15. Juli 2005
- Englisch
- ISBN-13: 9780470014301
- Artikelnr.: 37289844
- Verlag: John Wiley & Sons
- Seitenzahl: 292
- Erscheinungstermin: 15. Juli 2005
- Englisch
- ISBN-13: 9780470014301
- Artikelnr.: 37289844
William Henderson is the author of Mass Spectrometry of Inorganic and Organometallic Compounds: Tools - Techniques - Tips, published by Wiley. J. Scott McIndoe is the author of Mass Spectrometry of Inorganic and Organometallic Compounds: Tools - Techniques - Tips, published by Wiley.
Preface. List of commonly-used abbreviations. 1. Fundamentals. 1.1
Introduction. 1.2 Inlets. 1.3 Collision-induced dissociation. 1.4
Detectors. 1.5 Mass resolution. 1.6 Data processing. 1.7 Isotopes.
References. 2. Mass analysers. 2.1 Introduction. 2.2 Sectors. 2.3
Quadrupoles. 2.4 Quadrupole Ion Trap. 2.5 Time-of-flight. 2.6 Fourier
Transform Ion Cyclotron Resonance. References. 3. Ionisation techniques.
3.1 Introduction. 3.2 Electron ionisation. 3.3 Chemical Ionisation. 3.4
Field ionisation / Field desorption. 3.5 Plasma Desorption. 3.6 Fast Atom
Bombardment / Liquid Secondary Ion Mass Spectrometry. 3.7 Matrix Assisted
Laser Desorption Ionisation. 3.8 Inductively Coupled Plasma Mass
Spectrometry. 3.9 Electrospray ionisation. References. 4. The ESI MS
behaviour of simple inorganic compounds. 4.1 Introduction. 4.2 Simple metal
salts. 4.3 Polyanions formed by main group elements. 4.4 Oxoanions formed
by main group elements. 4.5 Borane anions. 4.6 Fullerenes. 4.7 Inorganic
phosphorus compounds: phosphoranes and cyclophosphazenes. 4.8 Summary.
References. 5. The ESI MS behaviour of coordination complexes. 5.1
Introduction. 5.2 Charged, "simple" coordination complexes. 5.3 (Neutral)
metal halide coordination complexes. 5.4 Metal complexes of polydentate
oxygen donor ligands: polyethers, crown ethers, cryptands and calixarenes.
5.5 Porphyrins and metalloporphyrins. 5.6 Metal alkoxides - highly
moisture-sensitive coordination compounds. 5.7 b-Diketonate complexes. 5.8
Metal complexes of carbohydrates. 5.9 Metal complexes of amino acids,
peptides and proteins. 5.10 Oxoanions, polyoxoanions and related species.
5.11 Metal clusters. 5.12 Compounds with anionic sulfur and selenium donor
ligands. 5.13 Characterisation of metal-based anticancer drugs, their
reaction products and metabolites. 5.14 In situ formation of coordination
complexes as an ionisation technique. 5.15 Summary. References. 6. The ESI
MS behaviour of main group organometallic compounds. 6.1 Introduction. 6.2
Organometallic derivatives of group 14 elements. 6.3 Organometallic
derivatives of group 15 elements. 6.4 Organometallic derivatives of group
16 elements; organo-sulfur, -selenium and -tellurium compounds. 6.5
Organomercury compounds. 6.6 Other organometallic derivatives. 6.7 Summary.
References. 7. The ESI MS behaviour of transition metal and lanthanide
organometallic compounds. 7.1 Introduction. 7.2 Metal carbonyl complexes.
7.3 Metal isocyanide complexes. 7.4 Metal cyclopentadienyl and related
complexes. 7.5 Metal h3-allyl complexes. 7.6 Metal arene complexes. 7.7
Formation of p-hydrocarbon complexes and their use as an ionisation aid.
7.8 Metal-acetylene/acetylide complexes, and complexes of metal-acetylides.
7.9 Transition metal s-alkyl and aryl complexes. 7.10 Mass spectrometry of
lanthanide organometallic complexes. 7.11 Summary. References. 8. A
selection of special topics. 8.1 Introduction. 8.2 Characterisation of
dendrimers using ESI and MALDI-TOF MS techniques. 8.3 Investigating the
formation of supramolecular coordination assemblies using ESI MS. 8.4 Using
ESI MS as a tool for directing chemical synthesis: A case studyinvolving
the platinum metalloligands [Pt2(m-E)2(PPh3)4] (E = S, Se). 8.5
Applications of ESI MS in the detection of reactive intermediates and
catalyst screening. References. Appendix 1: Naturally occurring isotopes.
Appendix 2: Periodic table of the elements. Appendix 3: Alphabetical list
of elements. Appendix 4: Glossary of Terms. Appendix 5: Useful sources of
information. Index.
Introduction. 1.2 Inlets. 1.3 Collision-induced dissociation. 1.4
Detectors. 1.5 Mass resolution. 1.6 Data processing. 1.7 Isotopes.
References. 2. Mass analysers. 2.1 Introduction. 2.2 Sectors. 2.3
Quadrupoles. 2.4 Quadrupole Ion Trap. 2.5 Time-of-flight. 2.6 Fourier
Transform Ion Cyclotron Resonance. References. 3. Ionisation techniques.
3.1 Introduction. 3.2 Electron ionisation. 3.3 Chemical Ionisation. 3.4
Field ionisation / Field desorption. 3.5 Plasma Desorption. 3.6 Fast Atom
Bombardment / Liquid Secondary Ion Mass Spectrometry. 3.7 Matrix Assisted
Laser Desorption Ionisation. 3.8 Inductively Coupled Plasma Mass
Spectrometry. 3.9 Electrospray ionisation. References. 4. The ESI MS
behaviour of simple inorganic compounds. 4.1 Introduction. 4.2 Simple metal
salts. 4.3 Polyanions formed by main group elements. 4.4 Oxoanions formed
by main group elements. 4.5 Borane anions. 4.6 Fullerenes. 4.7 Inorganic
phosphorus compounds: phosphoranes and cyclophosphazenes. 4.8 Summary.
References. 5. The ESI MS behaviour of coordination complexes. 5.1
Introduction. 5.2 Charged, "simple" coordination complexes. 5.3 (Neutral)
metal halide coordination complexes. 5.4 Metal complexes of polydentate
oxygen donor ligands: polyethers, crown ethers, cryptands and calixarenes.
5.5 Porphyrins and metalloporphyrins. 5.6 Metal alkoxides - highly
moisture-sensitive coordination compounds. 5.7 b-Diketonate complexes. 5.8
Metal complexes of carbohydrates. 5.9 Metal complexes of amino acids,
peptides and proteins. 5.10 Oxoanions, polyoxoanions and related species.
5.11 Metal clusters. 5.12 Compounds with anionic sulfur and selenium donor
ligands. 5.13 Characterisation of metal-based anticancer drugs, their
reaction products and metabolites. 5.14 In situ formation of coordination
complexes as an ionisation technique. 5.15 Summary. References. 6. The ESI
MS behaviour of main group organometallic compounds. 6.1 Introduction. 6.2
Organometallic derivatives of group 14 elements. 6.3 Organometallic
derivatives of group 15 elements. 6.4 Organometallic derivatives of group
16 elements; organo-sulfur, -selenium and -tellurium compounds. 6.5
Organomercury compounds. 6.6 Other organometallic derivatives. 6.7 Summary.
References. 7. The ESI MS behaviour of transition metal and lanthanide
organometallic compounds. 7.1 Introduction. 7.2 Metal carbonyl complexes.
7.3 Metal isocyanide complexes. 7.4 Metal cyclopentadienyl and related
complexes. 7.5 Metal h3-allyl complexes. 7.6 Metal arene complexes. 7.7
Formation of p-hydrocarbon complexes and their use as an ionisation aid.
7.8 Metal-acetylene/acetylide complexes, and complexes of metal-acetylides.
7.9 Transition metal s-alkyl and aryl complexes. 7.10 Mass spectrometry of
lanthanide organometallic complexes. 7.11 Summary. References. 8. A
selection of special topics. 8.1 Introduction. 8.2 Characterisation of
dendrimers using ESI and MALDI-TOF MS techniques. 8.3 Investigating the
formation of supramolecular coordination assemblies using ESI MS. 8.4 Using
ESI MS as a tool for directing chemical synthesis: A case studyinvolving
the platinum metalloligands [Pt2(m-E)2(PPh3)4] (E = S, Se). 8.5
Applications of ESI MS in the detection of reactive intermediates and
catalyst screening. References. Appendix 1: Naturally occurring isotopes.
Appendix 2: Periodic table of the elements. Appendix 3: Alphabetical list
of elements. Appendix 4: Glossary of Terms. Appendix 5: Useful sources of
information. Index.
Preface. List of commonly-used abbreviations. 1. Fundamentals. 1.1
Introduction. 1.2 Inlets. 1.3 Collision-induced dissociation. 1.4
Detectors. 1.5 Mass resolution. 1.6 Data processing. 1.7 Isotopes.
References. 2. Mass analysers. 2.1 Introduction. 2.2 Sectors. 2.3
Quadrupoles. 2.4 Quadrupole Ion Trap. 2.5 Time-of-flight. 2.6 Fourier
Transform Ion Cyclotron Resonance. References. 3. Ionisation techniques.
3.1 Introduction. 3.2 Electron ionisation. 3.3 Chemical Ionisation. 3.4
Field ionisation / Field desorption. 3.5 Plasma Desorption. 3.6 Fast Atom
Bombardment / Liquid Secondary Ion Mass Spectrometry. 3.7 Matrix Assisted
Laser Desorption Ionisation. 3.8 Inductively Coupled Plasma Mass
Spectrometry. 3.9 Electrospray ionisation. References. 4. The ESI MS
behaviour of simple inorganic compounds. 4.1 Introduction. 4.2 Simple metal
salts. 4.3 Polyanions formed by main group elements. 4.4 Oxoanions formed
by main group elements. 4.5 Borane anions. 4.6 Fullerenes. 4.7 Inorganic
phosphorus compounds: phosphoranes and cyclophosphazenes. 4.8 Summary.
References. 5. The ESI MS behaviour of coordination complexes. 5.1
Introduction. 5.2 Charged, "simple" coordination complexes. 5.3 (Neutral)
metal halide coordination complexes. 5.4 Metal complexes of polydentate
oxygen donor ligands: polyethers, crown ethers, cryptands and calixarenes.
5.5 Porphyrins and metalloporphyrins. 5.6 Metal alkoxides - highly
moisture-sensitive coordination compounds. 5.7 b-Diketonate complexes. 5.8
Metal complexes of carbohydrates. 5.9 Metal complexes of amino acids,
peptides and proteins. 5.10 Oxoanions, polyoxoanions and related species.
5.11 Metal clusters. 5.12 Compounds with anionic sulfur and selenium donor
ligands. 5.13 Characterisation of metal-based anticancer drugs, their
reaction products and metabolites. 5.14 In situ formation of coordination
complexes as an ionisation technique. 5.15 Summary. References. 6. The ESI
MS behaviour of main group organometallic compounds. 6.1 Introduction. 6.2
Organometallic derivatives of group 14 elements. 6.3 Organometallic
derivatives of group 15 elements. 6.4 Organometallic derivatives of group
16 elements; organo-sulfur, -selenium and -tellurium compounds. 6.5
Organomercury compounds. 6.6 Other organometallic derivatives. 6.7 Summary.
References. 7. The ESI MS behaviour of transition metal and lanthanide
organometallic compounds. 7.1 Introduction. 7.2 Metal carbonyl complexes.
7.3 Metal isocyanide complexes. 7.4 Metal cyclopentadienyl and related
complexes. 7.5 Metal h3-allyl complexes. 7.6 Metal arene complexes. 7.7
Formation of p-hydrocarbon complexes and their use as an ionisation aid.
7.8 Metal-acetylene/acetylide complexes, and complexes of metal-acetylides.
7.9 Transition metal s-alkyl and aryl complexes. 7.10 Mass spectrometry of
lanthanide organometallic complexes. 7.11 Summary. References. 8. A
selection of special topics. 8.1 Introduction. 8.2 Characterisation of
dendrimers using ESI and MALDI-TOF MS techniques. 8.3 Investigating the
formation of supramolecular coordination assemblies using ESI MS. 8.4 Using
ESI MS as a tool for directing chemical synthesis: A case studyinvolving
the platinum metalloligands [Pt2(m-E)2(PPh3)4] (E = S, Se). 8.5
Applications of ESI MS in the detection of reactive intermediates and
catalyst screening. References. Appendix 1: Naturally occurring isotopes.
Appendix 2: Periodic table of the elements. Appendix 3: Alphabetical list
of elements. Appendix 4: Glossary of Terms. Appendix 5: Useful sources of
information. Index.
Introduction. 1.2 Inlets. 1.3 Collision-induced dissociation. 1.4
Detectors. 1.5 Mass resolution. 1.6 Data processing. 1.7 Isotopes.
References. 2. Mass analysers. 2.1 Introduction. 2.2 Sectors. 2.3
Quadrupoles. 2.4 Quadrupole Ion Trap. 2.5 Time-of-flight. 2.6 Fourier
Transform Ion Cyclotron Resonance. References. 3. Ionisation techniques.
3.1 Introduction. 3.2 Electron ionisation. 3.3 Chemical Ionisation. 3.4
Field ionisation / Field desorption. 3.5 Plasma Desorption. 3.6 Fast Atom
Bombardment / Liquid Secondary Ion Mass Spectrometry. 3.7 Matrix Assisted
Laser Desorption Ionisation. 3.8 Inductively Coupled Plasma Mass
Spectrometry. 3.9 Electrospray ionisation. References. 4. The ESI MS
behaviour of simple inorganic compounds. 4.1 Introduction. 4.2 Simple metal
salts. 4.3 Polyanions formed by main group elements. 4.4 Oxoanions formed
by main group elements. 4.5 Borane anions. 4.6 Fullerenes. 4.7 Inorganic
phosphorus compounds: phosphoranes and cyclophosphazenes. 4.8 Summary.
References. 5. The ESI MS behaviour of coordination complexes. 5.1
Introduction. 5.2 Charged, "simple" coordination complexes. 5.3 (Neutral)
metal halide coordination complexes. 5.4 Metal complexes of polydentate
oxygen donor ligands: polyethers, crown ethers, cryptands and calixarenes.
5.5 Porphyrins and metalloporphyrins. 5.6 Metal alkoxides - highly
moisture-sensitive coordination compounds. 5.7 b-Diketonate complexes. 5.8
Metal complexes of carbohydrates. 5.9 Metal complexes of amino acids,
peptides and proteins. 5.10 Oxoanions, polyoxoanions and related species.
5.11 Metal clusters. 5.12 Compounds with anionic sulfur and selenium donor
ligands. 5.13 Characterisation of metal-based anticancer drugs, their
reaction products and metabolites. 5.14 In situ formation of coordination
complexes as an ionisation technique. 5.15 Summary. References. 6. The ESI
MS behaviour of main group organometallic compounds. 6.1 Introduction. 6.2
Organometallic derivatives of group 14 elements. 6.3 Organometallic
derivatives of group 15 elements. 6.4 Organometallic derivatives of group
16 elements; organo-sulfur, -selenium and -tellurium compounds. 6.5
Organomercury compounds. 6.6 Other organometallic derivatives. 6.7 Summary.
References. 7. The ESI MS behaviour of transition metal and lanthanide
organometallic compounds. 7.1 Introduction. 7.2 Metal carbonyl complexes.
7.3 Metal isocyanide complexes. 7.4 Metal cyclopentadienyl and related
complexes. 7.5 Metal h3-allyl complexes. 7.6 Metal arene complexes. 7.7
Formation of p-hydrocarbon complexes and their use as an ionisation aid.
7.8 Metal-acetylene/acetylide complexes, and complexes of metal-acetylides.
7.9 Transition metal s-alkyl and aryl complexes. 7.10 Mass spectrometry of
lanthanide organometallic complexes. 7.11 Summary. References. 8. A
selection of special topics. 8.1 Introduction. 8.2 Characterisation of
dendrimers using ESI and MALDI-TOF MS techniques. 8.3 Investigating the
formation of supramolecular coordination assemblies using ESI MS. 8.4 Using
ESI MS as a tool for directing chemical synthesis: A case studyinvolving
the platinum metalloligands [Pt2(m-E)2(PPh3)4] (E = S, Se). 8.5
Applications of ESI MS in the detection of reactive intermediates and
catalyst screening. References. Appendix 1: Naturally occurring isotopes.
Appendix 2: Periodic table of the elements. Appendix 3: Alphabetical list
of elements. Appendix 4: Glossary of Terms. Appendix 5: Useful sources of
information. Index.