Sabine Becker

Inorganic Mass Spectrometry (eBook, PDF)

Principles and Applications

• Format: PDF

Produktbeschreibung

Providing an exhaustive review of this topic, Inorganic Mass Spectrometry: Principles and Applications provides details on all aspects of inorganic mass spectrometry, from a historical overview of the topic to the principles and functions of mass separation and ion detection systems. Offering a comprehensive treatment of inorganic mass spectrometry, topics covered include: * Recent developments in instrumentation * Developing analytical techniques for measurements of trace and ultratrace impurities in different materials This broad textbook in inorganic mass spectrometry, presents the most important mass spectrometric techniques used in all fields of analytical chemistry. By covering recent developments and advances in all fields of inorganic mass spectrometry, this text provides researchers and students with information to answer any questions on this topic as well as providing the basic fundamentals for understanding this potentially complex, but increasingly relevant subject.

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Produktdetails

• Verlag: John Wiley & Sons
• Seitenzahl: 514
• Erscheinungstermin: 2. August 2008
• Englisch
• ISBN-13: 9780470517208
• Artikelnr.: 37294059

Autorenporträt

Johanna Sabine Becker; Since 1997- Deputy Head of Central Department for Analytical Chemistry, Research Centre Jülich.

Inhaltsangabe

Contents. Preface. Acknowledgement. Introduction to mass spectrometry. 1.
History of mass spectrometric techniques. 2. Ion sources. 2.1.Inductively
coupled plasma ion source. 2.2.Spark ion source. 2.3.Laser ion source.
2.4.Glow discharge ion source 2.5.Thermal surface ion source. 2.6. Ion
sources for secondary ion mass spectrometry (SIMS) and sputtered neutral
mass spectrometry (SNMS) 2.7.Electron impact ion source. 2.8.Matrix
assisted laser desorption/ ionization source. 2.9.Electrospray ion source.
3.Ion separation systems. 3.1 Sector field analyser. 3.2.Dynamic separation
systems. 3.3. Mass resolution and abundance sensitivity. 4. Ion detection
systems 4.1. Faraday cup. 4.2. Secondary electron multiplier. 4.3.
Combination of Faraday cup and secondary electron multiplier. 4.4. Channel
electron multiplier. 4.5. Daly detector. 4.6. Multiple ion collection
system. 4.7. Fluorescence screen and photographic ion detection.
5.Instrumentation 5.1. Inductively coupled plasma mass spectrometers
(ICP-MS). 5.2. Spark source mass spectrometers (SSMS) 5.3. Laser ionization
mass spectrometers (LIMS). 5.4. Resonance ionization mass spectrometers
(RIMS). 5.5. Glow discharge mass spectrometers (GDMS). 5.6. Termal
ionization mass spectrometers (TIMS). 5.7. Secondary ion mass spectrometers
(SIMS) and sputted neutral mass spectrometers.(SNMS). 5.8. Accelerator mass
spectrometers (AMS) 5.9. Electron impact mass spectrometers. 5.10. Knudsen
effusion mass spectrometers. 6. Analytical and practical considerations.
6.1. Qualitative analysis by inorganic mass spectrometry. 6.2.
Quantification procedures in inorganic mass spectrometry. 6.3. Sample
preparation and pretreatment in inorganic mass spectrometry. 7.Mass
spectrometric techniques for analysis of gaseous materials and volatile
compounds. 7.1. Sampling and sample preparation of gases and volatile
compounds 7.2. Applications of inorganic mass spectrometry for analysis of
gases and volatile compounds. 7.3. Stable isotope ratio measurements of
gases and volatile compounds. 8. Isotope ratio measurements and their
application 8.1. Capability of inorganic mass spectrometry in isotope ratio
measurements 8.2. Limits for precision and accuracy of isotope ratio
measurements and how to solve the problems 8.3. Isotope ratio measurements
by gas source mass spectrometry. 8.4. Isotope ratio measurements by
quadrupole based ICP-MS. 8.5. Isotope ratio measurements by laser ablation
ICP-MS 8.6. Multiple ion collector mass spectrometry for high precise
isotope ratio measurements 8.7. Application of isotope dilution technique
8.8. Isotope analysis of long-lived radionuclides 8.9. Application of
isotope ratio measurements in geochemistry and geochronology 9. Fields of
application of inorganic and mass spectrometry in trace, ultratrace and
surface analysis. 9.1. Material science. semiconductor technology 9.2.
Environmental science and environmental control. trace element species 9.3.
Biology. 9.4. Bioengineering 9.5.Medicine. 9.6. Food analysis. 9.7. Geology
and geochemistry. - U - Pb, Th - Pb and Pb-Pb methods for age dating. - Rb
- Sr method for age dating. - Sm-Nd method for age dating. - Lu-Hf-method
for age dating. - Re-Os-method for age dating - K-Ar/Ca-system for age
dating. - 14C dating 9.8. Cosmochemistry, planetary and space science.
9.9.Determination of long-lived radionuclides. 9.10. Forensic application.
9.11. Study of cluster and polyatomic ion formation by mass spectrometry.
9.12.Further applications. 10.Future developments. APPENDIX. Appendix
I:Table of isotopic abundances, atomic mass and ionization energies of
elements. Appendix II: Table of atomic weights of elements. Appendix III:
Definition. Appendix IV: Abbreviations and Acronyms. Appendix V: List of
standard reference materials for isotope ratio measurements.