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The objective and method of this thermal analysis of metal complexes book is to stimulate interest in research that will extend available theory towards a greater understanding of the steps involved in metal complexes decompositions, properties of metal complexes and decomposition kinetic parameter data consider with to calculate half decomposition temperature, Activation energy, Frequency factor, Entropy change and Free energy change. This book is designed to cover the "Thermal Analysis of Metal Complexes" use to calculate the different thermal method and water loss in chemical complexes. This book is applicable for Research student of Ph.D / M.E / M.Tech / M.Sc./ B.E./ B.Tech and all engineering, biochemical, biomedical, scientific courses and it provides various concepts of thermal Metal Complexes Chemistry with different thermograms and references. It cover up the recent need of thermal chemistry for Ph.D science research student, Industrial thermal worker, medical, biochemical and engineering courses as per requirement of Indian and various other universities and industry. This book explains the thermal analysis of metal complexes chemistry with three chapters.