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This book provides in depth explanation on Synthesis of FePt magnetic nanoparticles by Reverse micellar method. Characterization of FePt magnetic nanoparticles by Various techniques such as X-Ray fluorescence (XRF), Inductively coupled plasma optical emission spectroscopy (ICPOES),Differential Scanning Calorimetry (DSC), X-ray Diffraction (XRD),Vibrating Sample Magnetometer (VSM), Environmental Scanning Eletcron Microscopy (ESEM) and Transmission Eletcron Microscopy (TEM).