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Thin film science has received tremendous attention in last six decades especially after the word war-II, because of numerous and widespread applications of thin films in diverse fields such as electronic industries, micro-electronics and hybrid circuits, optical devices, sensors, superconductivity and recently high memory computer elements etc. This book entitled " Synthesis and Characterization of Bi2Se3 and Bi2-xPbxSe3 ternary compound thin film" covers the evaluation of particle size from Scherrer's formula, evaluation of optical band gap as well as optical constants such as refractive indices and extinction coefficient and photo-sensitivity nature of thin film.