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Techniques in Organic Chemistry is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students. It combines specific instructions for 3 different kinds of laboratory glassware (miniscale, standard-taper microscale and Williamson microscale) and offers extensive coverage of spectroscopic techniques, with a strong emphasis on safety issues.
Content:
PART 1: BASIC TECHNIQUES
Safety in the Laboratory and Protecting the Environment
Laboratory Glassware
The Laboratory Notebook
Using Handbooks and Online Databases
Measuring Volume
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Produktbeschreibung
Techniques in Organic Chemistry is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students. It combines specific instructions for 3 different kinds of laboratory glassware (miniscale, standard-taper microscale and Williamson microscale) and offers extensive coverage of spectroscopic techniques, with a strong emphasis on safety issues.

Content:
PART 1: BASIC TECHNIQUES
Safety in the Laboratory and Protecting the Environment
Laboratory Glassware
The Laboratory Notebook
Using Handbooks and Online Databases
Measuring Volume and Mass
Heating and Cooling Methods
Assembly of Reaction Apparatus and Planning Reactions
Extraction and Drying Organic Liquids
Recrystallization
Melting Points and Melting Ranges
Boiling Points and Distillation
Sublimation
Refractometry
Optical Activity and Polarimetry
PART 2: CHROMATOGRAPHY
Thin-Layer Chromatography
Gas-Liquid Chromatography
Liquid Chromatography
PART 3: SPECTROSCOPIC METHODS
Infrared Spectroscopy
Nuclear Magnetic Resonance Spectroscopy
Mass Spectrometry
Integrated Spectroscopy Problems
Appendix A Computational Chemistry
Appendix B The Literature of Organic Chemistry
Index
Autorenporträt
JERRY R. MOHRIG Carleton College, USA.

CHRISTINA NORING HAMMOND Vassar College, USA.

PAUL F. SCHATZ University of Wisconsin-Madison, USA.